Distillation Principles and Practice 2nd editon by Johann Stichlmair, Harald Klein, Sebastian Rehfeldt 1119414687 9781119414681

1 Introduction

1.1 Principle of Distillation Separation

1.2 Historical

References

2 Vapor–Liquid Equilibrium

2.1 Basic Thermodynamic Correlations

2.2 Calculation of Vapor–Liquid Equilibrium in Mixtures

2.3 Binary Mixtures and Phase Diagrams

2.4 Ternary Mixtures

References

Notes

3 Single‐Stage Distillation and Condensation

3.1 Continuous Closed Distillation and Condensation

3.2 Batchwise Open Distillation and Open Condensation

3.3 Semi‐continuous Single‐Stage Distillation

References

4 Multistage Continuous Distillation (Rectification)

4.1 Principles

4.2 Multistage Distillation of Binary Mixtures

4.3 Multistage Distillation of Ternary Mixtures

4.4 Multistage Distillation of Multicomponent Mixtures

References

5 Reactive Distillation, Catalytic Distillation

5.1 Fundamentals

5.2 Topology of Reactive Distillation Lines

5.3 Topology of Reactive Distillation Processes

5.4 Arrangement of Catalysts in Columns

References

6 Multistage Batch Distillation

6.1 Batch Distillation of Binary Mixtures

6.2 Batch Distillation of Ternary Mixtures

6.3 Batch Distillation of Multicomponent Mixtures

6.4 Influence of Column Liquid Hold‐up on Batch Distillation

6.5 Processes for Separating Zeotropic Mixtures by Batch Distillation

6.6 Processes for Separating Azeotropic Mixtures by Batch Distillation

References

7 Energy Economization in Distillation

7.1 Energy Requirement of Single Columns

7.2 Optimal Separation Sequences of Ternary Distillation

7.3 Modifications of the Basic Processes

7.4 Design of Heat Exchanger Networks

References

8 Industrial Distillation Processes

8.1 Constraints for Industrial Distillation Processes

8.2 Fractionation of Binary Mixtures

8.3 Fractionation of Multicomponent Zeotropic Mixtures

8.4 Fractionation of Heterogeneous Azeotropic Mixtures

8.5 Fractionation of Azeotropic Mixtures by Pressure Swing Processes

8.6 Fractionation of Azeotropic Mixtures by Addition of an Entrainer

8.7 Industrial Processes of Reactive Distillation

References

9 Design of Mass Transfer Equipment

9.1 Types of Design

9.2 Design of Tray Columns

9.3 Design of Packed Columns

Appendix

References

10 Control of Distillation Processes

10.1 Control Loops

10.2 Single Control Tasks for Distillation Columns

10.3 Basic Control Configurations of Distillation Columns

10.4 Application Ranges of the Basic Control Configurations

10.5 Examples for Control Configurations of Distillation Processes

10.6 Control Configurations for Batch Distillation Processes

References

Notes

Index

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